%0 Journal Article
%A LI Jia-Lei
%A WANG Kun-Lun
%A ZHAO Xiu-Hua
%A ZU Yuan-Gang
%T Preparation, Characterization and Function Evaluation of Ultrafine Resveratrol Powder
%D 2015
%R 10.7525/j.issn.1673-5102.2015.03.024
%J Bulletin of Botanical Research
%P 471-475
%V 35
%N 3
%X By supercritical SAS, we made the resveratrol anti solvent recrystallization to prepare ultrafine resveratrol powder under supercritical condition. The conditions were under 50℃, 20 MPa, resveratrol ethanol solution concentration of 9 mg·mL-1, and sample solution flow rate of 1 mL·min-1. We analyzed the particles by Dynamic Light Scattering(DLS) equipment and Scanning Electron Microscopy(SEM). The particle size of the particles was greatly reduced and the average particle size was 0.68±0.03 μm. In addition, characterization of ultrafine Res and raw-resveratrol were tested by Fourier transform infrared spectroscopy(FT-IR), X-ray diffraction(XRD), High performance liquid chromatography(HPLC) and Liquid chromatography-mass spectrometry(LC-MS). SAS process didn't change the chemical structure of Res. The chemical structure of resveratrol was unaffected by the SAS process. The degree of crystallinity of the u-Res particles greatly reduced. We used the purity of the u-Res particles increased from 98.5% to 99.2% during the SAS process. Using drosophila anti-aging experiments to detect the oxidation resistance of resveratrol. The antioxidant capacity of resveratrol powder were higher than that in the second-stage and blank experiment under the concentration of resveratrol solution, 2.5, 5 and 10 mg·mL-1. The resveratrol had the oxidation resistance, and ultrafine resveratrol powder was better than raw-resveratrol powder.
%U https://bbr.nefu.edu.cn/EN/10.7525/j.issn.1673-5102.2015.03.024